These are dichloro triazine reactive dyes. These dyes are highly reactive and hence does not require strong condition for fixation with cellulose material. These dyes are suitable for both dyeing and printing methods. |
| Dyeing Methods |
| • Exhaust Dyeing Method |
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| Diagram not to scale |
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Minutes |
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| Set temperature at 30°c |
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Load machine with the goods. Ensure that
pH is below 7. Adjust with acetic acid if necessary |
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05 |
add predissolved Dye |
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10 |
continue dyeing at 30°c |
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02 |
add 2.5 g/l Salt |
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10 |
continue dyeing at 30°c |
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03 |
add 7.5 g/l Salt |
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15 |
continue dyeing at 30°c |
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05 |
add remaining Salt |
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15 |
continue dyeing at 30°c |
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05 |
add 2.5 g/l Soda Ash slowly |
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15 |
continue dyeing at 30°c |
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05 |
add remaining Soda Ash |
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30-45 |
dye at 30°c
check shade |
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| Back to Top |
| • Jigger Dyeing Process |
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- Set the bath at 30-40° c
- Add dissolved dye over 2 ends
- Add salt over 2 ends, run for a minimum 30 minutes ( 2 ends or More )
- Add Alkali over 2 ends
- Run for a further 30-60 minutes ( 4 ends or More )
- Rinse thoroughly and wash off
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| Notes :
With ' difficult' materials it may be advantageous to dye at 50°c.
Raise temperature to 60°c for the last 20 minutes if Blue MGN used in mixtures |
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| • Salt and alkali requirement |
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% Shade |
Salt |
Soda Ash |
| Below 0.5% |
30 gms/l |
5 |
| 0.5 - Below 2% |
40 gms/l |
10 |
| 2.0 - below 4% |
50 gms/l |
15 |
| Above 4% |
60 gms/l |
20 |
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Camective dyes can be dyed by following two methods using Padding Mangle. |
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| • Pad Batch Process |
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| Camective M dyes X g/l |
| Alkali See table |
| Wetting agent 0.5 g/l |
| Urea 50-200g/l (if required for solubility ) |
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| 2-4 hours or 24 hours |
| ( See table below for alternatives ) |
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| Padding Method |
Padding GPL |
Sodium Bi-carbonate GPL |
Soda Ash GPL |
| Camective M' Dyes, |
0-5 |
- |
5 |
| 2-4 Hrs. batching |
5-30 |
- |
Equal to weight of dye |
| Cotton or Linen |
> 30 |
- |
30 |
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| Camective M' Dyes, |
0-5 |
4 |
1 |
| 24 Hrs. batching |
5-30 |
4/5 weight of dye |
1/5 weight of dye |
| Cotton or Linen |
> 30 |
20 |
10 |
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| Blue MGN and |
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| its Mixture |
0-5 |
- |
5 |
| 24 Hrs. batching |
5-30 |
- |
Equal to weight of dye |
| Cotton or Linen |
> 30 |
- |
30 |
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| Back to Top |
| • Pad Dry Process |
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| Camective M dyes X g/l |
| Sodium Bi-Carbonate |
5g/l (for Xg/I less then Sg/I) |
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10g/l (for Xg/t above 5g/l) |
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| Wetting agent 0.5 g/l |
| Urea 0-200g/l (if required for solubility ) |
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| 2-4 hours or 24 hours |
| ( See table below for alternatives ) |
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| • Printing Methods |
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Due to high reactivity of Camective M dyes the print paste stability is only a few hours and normally hydrolysis starts which leads to loss in colour strength. Hence care must be taken that printing is done as fast as possible after addition of Alkali. Different Printing Methods are
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(a) Print - dry - steam - wash - dry. |
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| Recipe |
Camective M' Dyes |
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X Part |
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Urea |
- |
50-75 Parts |
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Sodium Alginate (4%) |
- |
400 Parts |
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Resist Salt |
- |
10 Parts |
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Soda-bicarbonate |
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10-12.5 Parts |
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Water |
- |
Rest |
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Total |
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1000 Parts |
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Process :- The Dye is mixed with urea and warm water is added and stirred well till dye dissolves completely. To this solution mixture of sodium alginate and Resist salt is added and stirred well just prior to printing. Pre dissolved soda bicarbonate is added and printing is done immediately to avoid any colour loss. Print the fabric with above paste and dry. The Prints must be evenly dried and care must be taken that they do not come in contact with acid fumes. Then steam the dried goods on rapid ager for 1 minute or similar equipment. The fabric is then given after treatment. |
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| (b) Print - Dry - Bake - Wash - Dry |
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| Recipe |
Camective M' Dyes |
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X Part |
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Urea |
- |
150 Parts |
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Sodium Alginate (4%) |
- |
400 Parts |
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Resist Salt |
- |
10 Parts |
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Sodium-bicarbonate |
- |
15 Parts |
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Water |
- |
Rest |
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Total |
- |
1000 Parts |
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The process is similar to method (a) and baked here by as per the chart below. |
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Cotton |
Viscose |
| Temperature |
100° c |
200° c |
140° c |
200° c |
| Time |
3 minutes |
1 minute |
3 minutes |
1 minute |
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The goods are finally given after treatment. |
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(C) Print - Dry - Nippad - Dry - Wash - Dry |
The recipe is same as per method (a) except that instead of sodium bicarbonate soda ash 20g/l is used. The fabric is printed and dried. After drying the goods must not be stored for more time. The goods are then padded with solution containing 20 g/l soda ash. The padded goods are then dried on stenter or drying range, and then necessary after treatments are given. |
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(D) Pad - Dry - Print -Hang - Wash - Dry |
The recipe is same as in method (a) except that instead of soda bi-carbonate Soda ash is used. This method is for low end market where steaming and drying facility are not available, generally for hand processing units. In this method fabric is padded with solution of soda ash (20 g/l) and dried. The dried fabric is then printed with the print paste and dried by hanging in the open sunlight for about 5-6 hours During this drying condition fixation of dye takes place. The goods are then washed and dried. |
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| (E) Print - Dry - Pad Batch - Wash - Dry |
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| Recipe |
Camective M' Dyes |
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X Part |
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Urea |
- |
100 Parts |
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Sodium Alginate (4%) |
- |
400 Parts |
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Resist Salt |
- |
10 Parts |
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Water |
- |
Rest |
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Total |
- |
1000 Parts |
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In this method the goods are first printed with the print paste and dried. It is then padded through sodium-silicate solution of 100 - 102°Tw and batched for 45 minutes. It is then washed and dried.
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| General Washing Method |
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In order to achieve maximum fastness properties a proper wash off is essential
for the dyed and printed goods. |
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| Minutes |
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| 10 |
Rinse Cold |
| 10 |
Rinse Warm |
| 15-30 |
Soap at the boil. For Very heavy depth shades soaping required twice. |
| 10 |
Rinse Warm |
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Rinse Cold until clear solution is obtained. |
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For Medium to heavy shades an after treatment with 1 - 2 g/l dye fixing agent is
given at room temperature (40°C at acidic pH of 5 - 5.5 to improve fastness properties.) |
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YELLOW M4G
Reactive
Yellow 22 |
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YELOW M8G
Reactive
Yellow 86 |
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YELLOW MGR
Reactive
Yellow 7 |
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G. YELOW MR
Reactive
Yellow 44 |
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YELLOW MX4R
Reactive Orange 14 |
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YELOW M3R
Reactive
Orange 86 |
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ORANGE M2R
Reactive
Orange 4 |
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RED M5B
Reactive
Red 2 |
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RED M8B
Reactive
Red 11 |
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BLUE MR
Reactive
Blue 4 |
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NAVY BLUE M3R
Reactive
Blue 9
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BLUE M2R
Reactive
Blue 81 |
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BLUE MGN
Reactive
Blue 140 |
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BLUE MX7R
Reactive
Blue 161 |
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BLUE M4GD
Reactive
Blue 168 |
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VIOLET C4R
Reactive
Violet 12
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MEGENTA MB
Reactive
Violet 13 |
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